1-PHENYL-2-BUTANONE CAS NO.1007-32-5

Product Name:    1-PHENYL-2-BUTANONE
Synonyms:    2-Butanone, 1-phenyl-;2-Oxo-1-phenylbutane;Banzylethylketone;1-PHENYL-2-BUTANONE;ETHYL BENZYL KETONE;BENZYL ETHYL KETONE;1-phenylbutan-2-one;1-Phenylbutane-2-one
CAS:    1007-32-5                  
MF:    C10H12O                                                 
MW:    148.2         
EINECS:    213-752-1                       
Mol File:    1007-32-5.mol       

1-PHENYL-2-BUTANONE Chemical Properties
Melting point     72-73 °C
Boiling point     109-112 °C/15 mmHg (lit.)
density     0.998 g/mL at 25 °C (lit.)
refractive index     n20/D 1.512(lit.)
Fp     195 °F
storage temp.     2-8°C
form     Liquid
color     Clear colorless
BRN     1100022
CAS DataBase Reference    1007-32-5(CAS DataBase Reference)
Safety Information
Hazard Codes     Xn
Risk Statements     22
WGK Germany     3
HS Code     29143990
MSDS Information
Provider    Language
SigmaAldrich    English
1-PHENYL-2-BUTANONE Usage And Synthesis
Chemical Properties    Pale yellow oily liquid
Synthesis Reference(s)    Tetrahedron Letters, 23, p. 4167, 1982 DOI: 10.1016/S0040-4039(00)88377-X
Purification Methods    Purify the ketone by fractionation using an efficient column. It can be converted into the oxime which is distilled, b 117-118o/2mm, 145-146o/15mm, d 25 1.036, n D 1.5363; decompose the oxime, and the ketone is redistilled. It can also be purified via the semicarbazone which has m 154-155o. [Meyers et al. J Am Chem Soc 77 5655 1955, Hass et al. J Org Chem 15 8 1950, Beilstein 7 IV 712.]
1-PHENYL-2-BUTANONE Preparation Products And Raw materials
Raw materials    Thorium dioxide