ANILINE HYDROBROMIDE CAS NO.542-11-0

Product Name:    ANILINE HYDROBROMIDE
Synonyms:    aniliniumbromide;benzenamine,hydrobromide;benzenaminehydrobromide;ANILINE HYDROBROMIDE;Aniline·hydrogen bromide;Phenylammonium bromide;C6H8NBr(PhABr)
CAS:    542-11-0
MF:    C6H8BrN
MW:    174.04
EINECS:    208-801-9
Product Categories:    
Mol File:    542-11-0.mol          

Melting point     285°C(dec.)(lit.)
EPA Substance Registry System    Aniline hydrobromide (542-11-0)
Safety Information
MSDS Information
ANILINE HYDROBROMIDE Usage And Synthesis
Purification Methods    Crystallise the hydrobromide from water or EtOH and dry it at 5mm over P2O5. Also recrystallise it four times from MeOH containing a few drops of conc HBr by addition of pet ether (b 60-70o), then dry it to constant weight over paraffin chips in vacuo [Gutbezahl & Grunwald J Am Chem Soc 75 559 1953]. It precipitates from EtOH solution on addition of Et2O, and the filtered solid is recrystallised from EtOH and dried in vacuo. [Buchanan et al. J Am Chem Soc 108 1537 1986, Beilstein 12 III 232.]

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